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Download Advanced Distillation Technologies: Design, Control and by Anton A. Kiss PDF

By Anton A. Kiss

Distillation has traditionally been the most approach for setting apart combos within the chemical method undefined. in spite of the fact that, regardless of the flexibleness and common use of distillation methods, they nonetheless stay super strength inefficient. elevated optimization and novel distillation thoughts can carry sizeable merits, not only by way of considerably decrease strength use, but in addition in lowering capital funding and enhancing eco-efficiency. whereas prone to stay the separation expertise of selection for the following few a long time, there's no doubt that distillation applied sciences want to make radical alterations as a way to meet the calls for of the energy-conscious society.

Advanced Distillation applied sciences: layout, keep an eye on and purposes gives a deep and vast perception into built-in separations utilizing non-conventional preparations, together with either present and upcoming method intensification applied sciences.

It includes:

  • Key recommendations in distillation technology
  • Principles of layout, regulate, sizing and economics of distillation
  • Dividing-wall column (DWC) – layout, configurations, optimum operation and effort effective and complex control
  • DWC purposes in ternary separations, azeotropic, extractive and reactive distillation
  • Heat built-in distillation column (HIDiC) – layout, gear and configurations
  • Heat-pump assisted functions (MVR, TVR, AHP, CHRP, TAHP and others)
  • Cyclic distillation know-how – thoughts, modeling procedure, layout and keep watch over issues
  • Reactive distillation – basics, gear, purposes, feasibility scheme
  • Results of rigorous simulations in Mathworks Matlab & Simulink, Aspen Plus, Dynamics and customized Modeler

Containing plentiful examples and commercial case reports, this can be a targeted source that tackles the main complex distillation applied sciences – all of the means from the conceptual layout to useful implementation.

The writer of Advanced Distillation Technologies, Dr. Ir. Anton A. Kiss, has been presented the Hoogewerff Jongerenprijs 2013. discover extra (website in Dutch)...

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Additional resources for Advanced Distillation Technologies: Design, Control and Applications

Example text

Taylor, R. and Krishna, R. , New York. 1 INTRODUCTION This chapter provides the basic principles of design, control, sizing and economic estimates. Distillation is the most important thermal separation method used in the chemical process industry. Considering its many well-known benefits, distillation is and will certainly remain the separation method of choice in the chemical industry for the coming decades – with over 40 000 columns in operation worldwide. However, despite its flexibility and widespread use, one important drawback is the considerable energy requirements, as distillation can make up more than 50% of plant operating cost (Taylor, Krishna, and Kooijman, 2003).

Have higher relative volatilities) as temperature decreases – with some notable exceptions, as explained later. As a result, a low pressure is preferred in practice in order to provide low temperatures. Nevertheless, lower column pressures also give lower reflux-drum and condenser temperatures. While temperatures down to about 40–50  C can be achieved by using inexpensive cooling water, operating at temperatures lower than this range would require the use of chilled water or expensive refrigerant for the heat removal in the condenser.

Let us also assume that the reflux ratio has been specified, so the reflux flow rate can be calculated R ¼ RRD. The equimolar overflow assumption is usually made in the McCabe–Thiele method. The liquid and 28 ADVANCED DISTILLATION TECHNOLOGIES vapor flow rates are assumed to be constant in a given section of the column. For example, the liquid flow rate in the rectifying section LR is equal to the reflux flow rate R. From an overall balance around the top of the column, the vapor flow rate in the rectifying section VR is equal to the reflux plus the distillate (VR ¼ R þ D).

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